ZHE闆堕爞绌烘彁鍙栧櫒闆剁┖闁撳紡钀冨彇瀹瑰櫒瑁濈疆
| 鍨� 铏�(h脿o)锛� | TC-501 |
| 鍫�(b脿o) 鍍�(ji脿)锛� |  |
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- 鐢�(ch菐n)鍝佹弿杩�
ZHE闆堕爞绌烘彁鍙栧櫒闆剁┖闁撳紡钀冨彇瀹瑰櫒瑁濈疆
TC-501鍨嬮浂闋傜┖鎻愬彇鍣�
(闆堕爞绌烘彁鍙栧櫒鍙堝悕闆堕爞绌鸿悆鍙栧櫒銆侀浂绌洪枔寮忚悆鍙栧鍣�)
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浜屻�佸煼(zh铆)琛屾(bi膩o)婧�(zh菙n)
HJ/T299-2007銆婂浐楂斿虎鐗� 娴稿嚭姣掓�ф蹈鍑烘柟娉� 纭吀纭濋吀娉曘��
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涓夈�佷富瑕佺壒榛�(di菐n)
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2銆侀棞(gu膩n)閸靛瘑灏侀厤浠堕噰鐢ㄥ劒(y艒u)璩�(zh矛)鏉愭枡锛屽彲杓曟澗妯ｅ搧瑁濊級鍜岄亷婵撅紝淇濊瓑浜嗙敘(ch菐n)鍝佹埃瀵嗘�у拰闃茶厫鑰愮敤鎬�
3銆佸収(n猫i)灞ゅ拰琛ㄩ潰寰彙闈㈤垗鍖栬檿鐞嗭紝鍦ㄤ娇鐢ㄩ亷绋嬩腑鐒″垎瀛愭孩鍑猴紝鍏�(n猫i)閮ㄦ椿濉炵Щ鍕�(d貌ng)杓曟澗
鍥涖�佹妧琛�(sh霉)鍙冩暩(sh霉)
鍨嬭櫉(h脿o) | TC-501鍨嬮浂闋傜┖鎻愬彇鍣� |
鏉愯唱(zh矛) | 316涓嶉姽閶� |
鑰愬 | 鈮�100psi(0.7MPa) |
瑕�(gu墨)鏍� | 瀹归噺550ml锛岀洿寰�90mm |
鑰愭韩 | 鍙暦(zh菐ng)鏈熸斁缃�4鈩�浣庢韩涓� |
澹撳姏琛� | 0-230psi(0-1.6MPa) |
寰瓟婵捐啘 | 鐩村緫90mm锛屽瓟寰�0.6渭m |
浜斻�侀厤缃竻鍠�
搴忚櫉(h脿o) | 鐢�(ch菐n)鍝佸悕绋� | 鍨嬭櫉(h脿o) | 鏁�(sh霉)閲� | 鍌欐敞 |
1 | 闆堕爞绌烘彁鍙栧櫒 | TC-501鍨� | 1鑷�(t谩i) | |
2 | 鎼楁 | 1鏍� | ||
3 | 婵剧恫(w菐ng) | Φ90 | 2鐗� | |
4 | 婵捐啘 | Φ90 | 1鐩� | |
5 | PU姘ｇ | Φ5脳8 | 3绫� | |
6 | 鍚堟牸璀� | 1浠� | ||
7 | 瑾槑鏇� | 1浠� | ||
8 | 鍞悗鏈嶅嫏(w霉)鎵胯鏇� | 1浠� |
鍏�佷娇鐢ㄦ柟娉�
1銆佸皣闆堕爞绌烘彁鍙栧櫒鐨勯爞钃嬬敤鎼楁灏囨椿濉炴帹鍑猴紝鍐嶄互钂搁ぞ姘存饯(r霉n)婵曟椿濉炲銆�
2銆佸皣娲诲鐢遍爞灞ゅ钩琛℃斁鍏ラ浂闋傜┖鎻愬彇鍣ㄤ腑锛屽悜涓嬫帹鑷宠窛涓婅搵1cm铏�(鐩殑鏄璁撴彁鍙栧櫒閲岄潰鏈夎冻澶犵殑绌洪枔鐩涙斁娑查珨)锛屽啀灏囧簳灞ら帠绶娿��
3銆佹斁鍏ヨ│妯ｏ紝鐒跺悗鏀句笂涓�鍊�(g猫)涓嶉姽閶兼烤缍�(w菐ng)锛屾妸鐢ㄨ秴绱旀按娼�(r霉n)婵曢亷鐨勬烤鑶�(90mm) 鏀惧叆绗竴鍊�(g猫)閶煎埗婵剧恫(w菐ng)鐨勪笂闈紝鐒跺悗鏀句笂绗簩鍊�(g猫)婵剧恫(w菐ng)锛岃鍚屽績鏀剧疆锛岄槻姝㈤尟(cu貌)浣嶃��
4銆佹斁涓婅搵瀛愶紝鐢ㄤ笁鍊�(g猫)铻虹挡鏃嬬穵鍥哄畾濂斤紝瑕佺壒鍒ユ敞鎰忓湪鏃嬬穵鐨勯亷绋嬩腑涓嶈兘鎶婂叾涓竴鍊�(g猫)铻虹挡鏃嬪埌鏈�绶婂啀鍘绘棆鍏朵粬铻虹挡锛岃璺熶笂娉曡槶鐩や技鐨勫洓鍊�(g猫)閫愭几鏃嬬穵锛岄槻姝㈢敘(ch菐n)鐢熺┖闅欒�屾紡姘ｃ��
5銆佸皣绱旀按鑸囨ǎ鍝佸姞鍏ュ鍣ㄥ悗锛屾妸闆堕爞绌烘彁鍙栧櫒涓婁笅闁ラ杸閮介棞(gu膩n)闁夛紝闆堕爡(xi脿ng)绌烘彁鍙栧櫒涓嬮潰姘ｅ槾鑸囨爱?d煤)鎬冩拡鍧戦湁鑼忚垎B鎺ュソ锛屾妸姘�?d煤)鎬冩拡鍙帵濞存媹y闁�鎵撻枊锛岀劧鍚庡啀鎵撻枊闆堕爞绌烘彁鍙栧櫒涓嬮潰鐨勯枼闁�锛岄枊濮嬬敤姘�?d煤)鎬冩拡鎷穙闆堕爞绌烘彁鍙栧櫒鍔犲锛岀湅闆堕爞绌烘彁鍙栧櫒澹撳姏琛ㄦ暩(sh霉)鍊奸仈(d谩)鍒�20psi(绱�0.14MPa)灏卞仠姝㈠姞澹擄紝闂�(gu膩n)闁夐浂闋傜┖鎻愬彇鍣ㄤ笅闈㈤枼闁�锛屾挙鎺夋爱?d煤)鎬冩拡娴氼兒@鏅�(sh铆)鎶婇浂闋傜┖鎻愬彇鍣ㄤ笂闈㈡埃鍢撮�ｄ笂涓�绡�(ji茅)纭呰啝绠★紝杓曡紩鏃嬪嫊(d貌ng)闁ラ杸涓婄殑钘�(l谩n)鑹叉棆閳�(娉ㄦ剰:涓�瀹氳杓曡紩鏃嬪嫊(d貌ng))锛岀暥(d膩ng)鐪嬪埌纭呰啝绠″嚭鐝�(xi脿n)姘存煴鏅�(sh铆)(瑾槑闆堕爞绌烘彁鍙栧櫒閲岄潰鐨勭┖姘ｅ凡缍�(j墨ng)鍏ㄩ儴闋傚嚭)锛岃繀閫熸棆杞�(zhu菐n)钘�(l谩n)鑹叉棆閳曪紝闂�(gu膩n)闁夐枼闁�銆�
6銆佸皣瀹屾垚浠ヤ笂姝ラ鍚庣殑闆堕爞绌烘彁鍙栧櫒鏀剧疆鍒扮炕杞�(zhu菐n)寮忔尟钑╁櫒涓婏紝娉ㄦ剰鎳�(y墨ng)浠ュ崄瀛楀舰灏�(du矛)绋辨柟寮忔斁缃紝骞舵敞鎰忓簳灞ら浂浠跺湪鏃嬭綁(zhu菐n)鏅�(sh铆)涓嶆渻(hu矛)纰版挒鍒板叾浠栫墿鍝侊紝涓斿懆鍦嶇挵(hu谩n)澧冧笉鏈�(hu矛)濡ㄧ鏃嬭綁(zhu菐n)鍣ㄧ殑鎿嶄綔銆傚苟浠�30±2杞�(zhu菐n)/min鐨勯�熷害鎸暕18±2h銆� 瀵�(sh铆)椹�(y脿n)瀹岀暍鍚庢妸闆堕爞绌烘彁鍙栧櫒鍙栦笅锛岄爞灞ら枊闂�(gu膩n)闁ユ墦闁嬪苟鎺ヤ笂姘ｅ瘑寮忔敞灏勫櫒锛屽緸搴曞堡绶╂參鍔犲锛岃畵娑查珨寰炴彁鍙栧櫒涓珐鎱㈡祦鍏ユ埃瀵嗗紡娉ㄥ皠鍣ㄤ腑锛屼笂杩板嫊(d貌ng)浣滀竴鐩存寔绾�(x霉)鍒伴爞灞ゅ嚭鍙ｄ笉鍐嶅啋鍑烘恫楂斿悗锛岄棞(gu膩n)闁夐爞灞ら枊闂�(gu膩n)骞舵嫈鎺夊簳灞ょ殑蹇�熸埃楂旀彃闋紝姝ゆ檪(sh铆)鏁村��(g猫)閬庢烤瀹屾垚銆�
涓冦�佹敞鎰忎簨闋�(xi脿ng)
8.1涓�鑸儏娉佷笅锛岄厤鍚堢炕杞�(zhu菐n)鎸暕鍣ㄤ娇鐢ㄦ檪(sh铆)闆堕爞绌烘彁鍙栧櫒瑕侀伕閰嶇洿寰戠偤90mm瀛斿緫0.6-0.8渭m鐨勫井瀛旀烤鑶滅偤浣炽��
8.2闆堕爞绌烘彁鍙栧櫒鍦ㄤ娇鐢ㄥ畬鐣㈠悗锛岃娉ㄦ剰娓呮礂骞插噲骞跺湪閬╃暥(d膩ng)?sh霉)娌玥(hu谩n)澧冧腑閫�(j矛n)琛屽瓨璨��
8.3鎶婇浂闋傜┖钀冨彇瀹瑰櫒鏀剧疆鍦ㄧ炕杞�(zhu菐n)鎸暕鍣ㄤ笂涔嬪墠锛屼竴瀹氳鎶婃墍鏈夌殑鏃嬮垥铻虹挡鐢ㄥ伐鍏峰姞鍥轰互闃茶灪绲茶劔钀姐��
8.4鐢ㄦ悧妫掑幓鎼楅浂闋傜┖钀冨彇瀹瑰櫒涓笉閵归嫾娲诲鏅�(sh铆)鎼楁鏈�濂芥斁鍦ㄦ椿濉炵殑涓績浣嶇疆锛屾渶濂界敤灏忛寴瀛愭暡鎿婃悧妫掋��
闄勶細妯�(bi膩o)婧�(zh菙n)涓厤濂楀剙鍣ㄨō(sh猫)鍌�
5鍎�鍣ㄨō(sh猫)鍌�
5.1鎸暕瑷�(sh猫)鍌欙細杞�(zhu菐n)閫熺偤30±2r/min鐨勭炕杞�(zhu菐n)寮忔尟钑╄缃��
5.2鎻愬彇瀹瑰櫒
5.2.1闆堕爞绌烘彁鍙栧櫒锛�Zero-Head space Extraction Vessel锛屼互涓嬬啊(ji菐n)绋�ZHE锛夛細500-600ml锛岀敤浜庢ǎ鍝佷腑鎻櫦(f膩)鎬х墿璩�(zh矛)娴稿嚭鐨勮缃��
5.2.2鎻愬彇鐡讹細2L鍏锋棆钃嬪拰鍏�(n猫i)钃嬬殑寤ｅ彛鐡讹紝鐢ㄤ簬娴稿嚭妯ｅ搧涓潪鎻櫦(f膩)鎬у拰鍗婃彯鐧�(f膩)鎬х墿璩�(zh矛)銆傛彁鍙栫摱鎳�(y墨ng)鐢变笉鑳芥蹈鍑烘垨鍚告敹妯ｅ搧鎵�鍚垚鍒嗙殑鎯版�ф潗鏂欏埗鎴愩�傚垎鏋愮劇姗�(j墨)鐗╂檪(sh铆)锛屽彲浣跨敤鐜荤拑鐡舵垨鑱氫箼鐑紙PE锛夌摱锛涘垎鏋愭湁姗�(j墨)鐗╂檪(sh铆)锛屽彲浣跨敤鐜荤拑鐡舵垨鑱氬洓姘熶箼鐑紙PTFE锛夌摱銆�
5.3閬庢烤瑁濈疆
5.3.1闆堕爞绌烘彁鍙栧櫒锛�ZHE锛夛細鍒嗘瀽妯ｅ搧涓殑鎻櫦(f膩)鎬х墿璩�(zh矛)锛岄噰鐢�ZHE閫�(j矛n)琛岄亷婵俱��
5.3.2鐪熺┖閬庢烤鍣ㄦ垨姝ｅ閬庢烤鍣細瀹圭⿳鈮�1L銆�
5.3.3婵捐啘锛氱幓绾栨烤鑶滄垨寰瓟婵捐啘锛屽瓟寰�0.6-0.8渭m銆�
5.4pH瑷�(j矛)锛氬湪25鏅�(sh铆)锛岀簿搴︾偤±0.05pH銆�
5.5ZHE娴稿嚭娑查噰闆嗚缃細浣跨敤ZHE瑁濈疆鏅�(sh铆)锛岄噰鐢ㄧ幓鐠冦�佷笉閵归嫾鎴�PTFE鍒朵綔鐨�500ml娉ㄥ皠鍣ㄩ噰闆嗗垵濮嬫恫鐩告垨绲傜殑娴稿嚭娑层��
5.6ZHE娴告彁鍔戣綁(zhu菐n)绉昏缃細鍙互浣跨敤浠讳綍涓嶆敼璁婃蹈鎻愬姂鎬ц唱(zh矛)鐨勫皫(d菐o)鍏ヨō(sh猫)鍌欙紝鍖呮嫭锠曞嫊(d貌ng)娉点�佹敞灏勫櫒銆佹澹撻亷婵惧櫒鎴栧叾瀹�ZHE瑁濈疆銆�
5.7瀵�(sh铆)椹�(y脿n)澶╁钩锛氱簿搴︾偤±0.01g銆�
5.8鐕掓澂鎴栭寪褰㈢摱锛氱幓鐠冿紝500ml銆�
5.9琛ㄩ潰鐨匡細鐩村緫鍙搵浣忕噿鏉垨閷愬舰鐡躲��
5.10绡╋細娑�Teflon鐨勭缍�(w菐ng)锛屽瓟寰�9.5mm銆�